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DMT StB Extraction Problems

  • Auteur de la discussion Auteur de la discussion randooo
  • Date de début Date de début
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randooo

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One of my buddies is doing an extraction using 2 separate 100g solutions of MHRB, lye and (purified) water. a few questions because he is too proud to ask for help on the internet. He used ~100g of powdered rootbark, ~100g of lye, and ~1750 ml of water, (prepowdered root bark takes more water). He followed http://www.erowid.org/plants/mimosa/mimosa_chemistry1.shtml this Tek. However, when he pulled the naptha off the top each time, the naptha was completely clear, no color whatsoever, then left in the freezer for going on 35 hours now. No crystals have formed. However, he had the jar CAPPED.
does he need to uncap the jar in the freezer? also, should the naptha have any color going into the freezer? and finally, does the fact that purified water was used make a difference?
the naptha was heated before putting it into the MHRB/NaOH/H20 solution, but the solution itself was not heated.
 
How much solvent did you use? Try evaporating it to see if it has collected anything maybe. Pretty sure the solvent (lighter fluid/naptha) went yellowy when AFOAF did it. Did you mix it up a few times and let it seperate? It's a hard one to mess up - maybe the root bark isn't right or low in alkoloids? What is your source for the naphtha?
 
Evaporate the solvent to about half the volume. Put in freezer again, doesn't matter if cap is on or off - better if it is off, but it will make your freezer smell of cancer.

You may be using way too much solvent.
 
was there a crazy emulsion, or did the two layers separate nicely?
 
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