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Please check my method for DMT extraction

  • Auteur de la discussion Auteur de la discussion Kent
  • Date de début Date de début

Kent

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My method for extracting DMT from Phalaris Arundinacea

Post by Kent » Thu Oct 21, 2010 22:05
I would like to list here the method I have used for extracting DMT from Phalaris Arundinacea.
I would like some feedback from experienced chemists and/or people that have done this before to be sure that the method I have used is safe and effective.

Ok first, I started off by pulverizing the Phalaris grass clippings into a nearly liquid form.
I then added enough water to make it into a pourable soup.
Then I added enough lemon juice to bring the ph down to about 5.5.
I then let it simmer on the stove for 8 hours.
After that I strained the soup through a coffee filter several times, and discarded the bulk from the plant material.
I then took super tech engine starting fluid and sprayed it down a long plastic vacuum tube, letting the liquid ether drip into the soup and the other vapors evaporate into the air.
I let the mixture sit for another 8 hours until the solvent layer had sunken to the bottom. (I was told that the solvent layer full of fats and oils would float to the top, but it didn't).
So instead of being able to simply remove the solvent layer, I had to strain the mixture through a coffee filter about 5 times.
Each time I strained it through the coffee filter, it would leave behind the darkbrown gunk that I would wash down the sink.
I then reused the coffee filter for the same process, repeating until there was no more brown gunk to discard.
Finally when the mixture was purified of the gunk, I added drain cleaner in small increments until the ph rose to about 9.
I then added more engine starting fluid, spraying it once again down the plastic tube and allowing the liquid ether to drip into the mixture. (I only added enough ether to equal 10% of the total mixture).
I then took the solution inside and sat it under the sink for 24 hours. There does seem to be a white crystalline substance rising to the top of the solution, so I'm thinking I did it right. But I thought it would be a good idea to consult more experienced extractors before testing the final product. :D
 
first... how much grass.

second...
I let the mixture sit for another 8 hours until the solvent layer had sunken to the bottom. (I was told that the solvent layer full of fats and oils would float to the top, but it didn't).
this doesn't sound good.
Did you test the ether solvent you used for purity? when it evaporates does it leave behind a residue?

I added drain cleaner
what drain cleaner... they don't make many drain cleaners that are ~100% NaOH anymore...

Your pH is too low to extract DMT i think.

I don't know what solvent you are using though... Would you mind typing in MSDS "Your engine starter fluid name" into google and telling me the main ingredients?

When all the extract is finished please tell me the smell of the purified, dry (no solvent left) crystal.
 
I used about 5 grams of pulverized phalaris grass.
I don't think the ether left behind any kind of residue.
I used Drain Power professional strength drain cleaner.
The engine starting fluid I used was Supertech engine starting fluid.
The main ingredients are Heptane, Ethyl Ether, Propane, Carbon Dioxide, Iso-Butane, and Lubricating Oil.
The end result was a yellowish white crystalline powder. I don't think it really had much of a smell. Besides maybe a slight chemical smell. But that was when I very first extracted it. It's actually not even done drying yet.
 
Lubricating Oil

This will not evaporate off, and your end product will end up inhaling this if you smoke it.

5 grams of phalaris will get you about a half a milligram of DMT to max 5 milligrams. Either way, not enough to smoke.

Sorry.
 
Thank you for your input. I will have to try again and next time do things differently.
 
If you are serious about investiing time & money into extracting from phalaris 2 things;

1. buy a wheat grass extractor.
2. tell us all how it goes. Keep some notes as to how things turn out and pass it on. Some serious research needs to be put into this method.
 
swim uses this method he sent it to me

" just soak 30-50g mimosa with 2cups water and 2ml muriatic acid or lemon juice or whatever acidifies it.
draw up some hot water in one side of your sink, and let it have a hot water bath for about half an hour, and be sure to relieve the pressure that will build up every once in a while.
all the while shake it every now and then.
then put it away for about a day
then get a funnel and cottonballs and plug up the bottom of the funnel
run the shit through that and keep the excess "gunk" and do another pull with it
2 pulls should get most of it
after you have 2 pulls of pure extracted purplist redish looking shit
you get some naphha or whatever solvent your using and warm it up then our it into the mix
then get a big cup of water and since i cant really measure this shit i dont have a scale
just get 2 cups of water and SLOWLY pour the "drano" into the water while stirring, and it should get hot,
dont pour in too much
when you feel it start to get warm thats probabbly enough..
then
you get your other mixture of solvent and mimosa extract and you start stirring it and adding the drano-water mixture VERY slowly, until it turns grey or blue, then it will turn brownish, then it will turn black... keep stirring it, maybe put a cap on it and shake it a bit, then if theirs an emulsion, add a tiny bit more drano-water mixture. then do the DMT shuffle
after about a day or two it should definitely have settled and be good get a turkey baster and suck up all the solvent off the top.
put it in a pan, you can either freeze it out or evap, freezing could make it more pure i think, but evap seems to be alot faster"
 
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